• 专利标题:   Preparation of electrode material used in supercapacitor, involves injecting ink prepared using e.g. molybdenum disulfide-carbon nanotube material and graphene oxide dispersion into coaxial printing needle, printing, drying and etching.
  • 专利号:   CN112992557-A, CN112992557-B
  • 发明人:   ZHANG Y, LV X, JIA S, LI Q, LIU M
  • 专利权人:   NANOTECH NANOBIONICS CHINESE ACADEMY, JIANGXI NANOTECHNOLOGY RES INST
  • 国际专利分类:   H01G011/26, H01G011/36, H01G011/86
  • 专利详细信息:   CN112992557-A 18 Jun 2021 H01G-011/86 202163 Pages: 13 Chinese
  • 申请详细信息:   CN112992557-A CN10166169 05 Feb 2021
  • 优先权号:   CN10166169

▎ 摘  要

NOVELTY - Preparation of molybdenum disulfide-carbon nanotube/graphene electrode material involves providing graphene oxide dispersion as an outer layer printing ink, synthesizing molybdenum disulfide in-situ on the surface of carbon nanotubes, obtaining molybdenum disulfide-carbon nanotube material, mixing the molybdenum disulfide-carbon nanotube material with carbon nanotubes and thickener, obtaining an inner layer printing ink, injecting inner layer printing ink and outer layer printing ink respectively into the inner and outer layers of a coaxial printing needle, performing three-dimensional coaxial wet printing process, freeze-drying obtained molybdenum disulfide-carbon nanotubes/graphene oxide coaxial fiber, and performing reduction etching treatment. USE - Preparation of molybdenum disulfide-carbon nanotube/graphene electrode material used in supercapacitor e.g. pseudocapacitance supercapacitor (all claimed). ADVANTAGE - The method enables economical preparation of molybdenum disulfide-carbon nanotube/graphene electrode material with high conductivity, specific capacitance and stability, and excellent rate performance, by simple and environmentally-friendly process. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the molybdenum disulfide-carbon nanotube/graphene electrode material, which comprises an inner layer of molybdenum disulfide-carbon nanotube material and an outer layer of reduced graphene oxide, which are coaxially provided. The content of molybdenum disulfide in the molybdenum disulfide-carbon nanotube/graphene electrode material is 50-80 wt.%.