• 专利标题:   Preparation method of defective graphene, involves lowering temperature after calcination is completed, replacing inert atmosphere with air atmosphere, and lowering temperature, after heat preservation to obtain defective graphene.
  • 专利号:   CN113896186-A
  • 发明人:   TAN W, JING M, LIU L, MA F
  • 专利权人:   UNIV SHANDONG JIANZHU
  • 国际专利分类:   C01B032/19, C01B032/194
  • 专利详细信息:   CN113896186-A 07 Jan 2022 C01B-032/19 202224 Chinese
  • 申请详细信息:   CN113896186-A CN11062152 10 Sep 2021
  • 优先权号:   CN11062152

▎ 摘  要

NOVELTY - The method involves weighing a certain mass of expandable graphite, putting into the bottom of the crucible, putting the crucible into the muffle furnace, and carrying out segmented calcination. The product in the crucible is taken out, and the graphene is obtained by high-speed crushing. The broken graphene is calcined in sections under the protection of an inert atmosphere. The temperature is lowered, after the calcination is completed, the inert atmosphere is replaced with an air atmosphere, and the temperature is naturally lowered, after heat preservation to obtain defective graphene. USE - Preparation method of defective graphene. ADVANTAGE - The method provides defect graphene with low cost and simple operation step in the drying environment, the reaction condition is convenient and controllable, and the needed device is simple. The preparation process is green and environment-friendly, and the defect graphene still keeps the original graphene structure, and only partial crystal lattice is absent. DESCRIPTION OF DRAWING(S) - The drawing shows a preparation process of the invention intermediate product graphene and defect graphene SEM photograph. (Drawing includes non-English language text).