• 专利标题:   Density gradient type high hydrogen storage composite film resistant to irradiation of charged particles prepared by e.g. adding zinc oxide film deposited on surface of cobalt sulfide metal compound into graphene, drying and hydrogenating.
  • 专利号:   CN111962046-A
  • 发明人:   WU X, LI Y, OU X, JIANG L, LI T, YANG X
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   C23C016/40, C23C016/455, C23C016/56
  • 专利详细信息:   CN111962046-A 20 Nov 2020 C23C-016/40 202003 Pages: 4 Chinese
  • 申请详细信息:   CN111962046-A CN10788669 07 Aug 2020
  • 优先权号:   CN10788669

▎ 摘  要

NOVELTY - Density gradient type high hydrogen storage composite film resistant to irradiation of charged particles is claimed. The composite protective film layer is a zinc oxide film deposited on the surface of the cobalt sulfide (Co9S8) metal compound, then adding it to the graphene, high-energy ball milling under protection of protective gas, adding acetone after taking it out, and ultrasonically dispersing to uniformity, adding 70-80 degrees C epoxy resin, stirring quickly at constant temperature of 70-80 degrees C until the acetone solvent evaporates completely, then adding the curing agent, magnetically stirring until the mixture is uniform, coating on the surface of the substrate with same surface density to form film, drying and then hydrogenating. USE - Used as density gradient type high hydrogen storage composite film resistant to irradiation of charged particles. ADVANTAGE - The composite film: adopts atomic layer deposition technology to deposit zinc oxide film on the surface of cobalt-sulfur metal compound, and then prepares high-hydrogen storage cobalt-sulfur metal compound through high-energy ball milling technology; improves bonding ability of hydrogen storage material and matrix. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing density gradient type high hydrogen storage composite film resistant to irradiation of charged particles. The method utilizes zinc source, substrate, oxygen source, curing agent, epoxy resin and acetone.