• 专利标题:   Preparation of graphene dispersion, involves adding monomer, initiator and solvent to reactor, drying, adding dried mixture, imidazole and solvent to reactor, removing solvent, adding obtained solid and graphene to solvent and centrifuging.
  • 专利号:   CN106915740-A, CN106915740-B
  • 发明人:   CHEN C, CHEN J, WAN J
  • 专利权人:   TBRIGHT JIANGSU NEW MATERIAL TECHNOLOG, TBRIGHT JIANGSU NEW MATERIAL TECHNOLOGY
  • 国际专利分类:   C01B032/194, C08F212/08, C08F212/14, C08F220/18, C08F220/28, C08F008/30
  • 专利详细信息:   CN106915740-A 04 Jul 2017 C01B-032/194 201765 Pages: 8 Chinese
  • 申请详细信息:   CN106915740-A CN10316437 08 May 2017
  • 优先权号:   CN10316437

▎ 摘  要

NOVELTY - Preparation of graphene dispersion, involves adding monomer, initiator and solvent (I) to reaction vessel, reacting, removing solvent (I) by distillation, drying to obtain linear polymer, adding obtained linear polymer to reaction vessel, adding solvent (II) to dissolve completely, adding N-methylimidazole to reaction vessel, stirring, heating, reacting, removing solvent (II) by distillation to obtain pale yellow solid, adding obtained solid and graphene powder to solvent (III), mixing, dispersing ultrasonically and carrying out centrifugal separation to obtain supernatant. USE - Preparation of graphene dispersion. ADVANTAGE - The method provides graphene dispersion, which has high concentration, excellent storage stability and electrical conductivity. DETAILED DESCRIPTION - Preparation of graphene dispersion, involves (a) adding reaction monomer, initiator and solvent (I) to reaction vessel, reacting under stirring at 110 degrees C, removing solvent (I) by distillation under reduced pressure, drying to obtain linear polymer, (b) adding obtained linear polymer to reaction vessel, adding solvent (II) to dissolve completely, adding N-methylimidazole dropwise to reaction vessel under stirring, heating continuously at 90 degrees C, reacting under nitrogen protection, removing solvent (II) by distillation under reduced pressure to obtain pale yellow solid, (c) adding obtained solid and graphene powder to solvent (III), mixing, dispersing ultrasonically and carrying out centrifugal separation to obtain supernatant.