• 专利标题:   Preparing magnetic graphene oxide surfactant comprises e.g. adding dimethylaminopropyl)-ethylcarbodiimide hydrochloride and polyethylene glycol to react, adding polyethylene glycol-wrapped magnetic graphene oxide and surfactant into solvent to react to obtain magnetic graphene oxide surfactant.
  • 专利号:   CN114574238-A, CN114574238-B
  • 发明人:   LI X, GUAN B, ZHENG X, PENG B, WANG Z, WANG Y, HOU Q
  • 专利权人:   PETROCHINA CO LTD
  • 国际专利分类:   C02F001/28, C02F001/40, C02F101/20, C02F101/32, C02F103/10, C09K008/584, C10G025/00, C10G033/04
  • 专利详细信息:   CN114574238-A 03 Jun 2022 C10G-033/04 202274 Chinese
  • 申请详细信息:   CN114574238-A CN11392611 02 Dec 2020
  • 优先权号:   CN11392611

▎ 摘  要

NOVELTY - Preparing magnetic graphene oxide surfactant comprises (1) mixing the graphene oxide, the iron source and the aqueous ammonia-ammonium nitrate solution and reacting to obtain magnetic graphene oxide, (2) dispersing the magnetic graphene oxide in deionized water, and adding 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride and polyethylene glycol to react to obtain magnetic graphene oxide wrapped with polyethylene glycol, and (3) adding the polyethylene glycol-wrapped magnetic graphene oxide and surfactant into solvent to react to obtain the magnetic graphene oxide surfactant. USE - The method is useful for preparing magnetic graphene oxide surfactant. ADVANTAGE - The method: can carry out graft modification of graphene oxide and surfactant under relatively mild conditions; can not only emulsify oil and water; quickly breaks demulsification under the condition of external magnetic field; and has certain adsorption effect on metal ions in oilfield produced fluid. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for magnetic graphene oxide surfactant obtained by the preparation method.