• 专利标题:   Preparation of composite material for e.g. photocatalytic degradation of organic compound, involves adding graphene oxide into mixed solution of water and organic solvent, stirring, adding silver nitrate aqueous solution, and stirring.
  • 专利号:   CN103551145-A
  • 发明人:   WANG M, GAO Y, RAN C
  • 专利权人:   UNIV XIAN JIAOTONG
  • 国际专利分类:   B01J023/50
  • 专利详细信息:   CN103551145-A 05 Feb 2014 B01J-023/50 201424 Chinese
  • 申请详细信息:   CN103551145-A CN10308861 22 Jul 2013
  • 优先权号:   CN10308861

▎ 摘  要

NOVELTY - Preparation of nano silver/graphene/P25 composite material involves adding graphene oxide into a mixed solution of water and organic solvent, ultrasonically dispersing, adding silver nitrate aqueous solution into obtained dispersion (A), magnetically stirring the mixture, adding P25-type powder into obtained nano silver/graphene oxide solution (B), stirring, reacting obtained nano silver/graphene oxide/P25 aqueous/organic solvent solution in an oil bath, cooling the reaction mixture to room temperature, filtering, washing, and vacuum-drying obtained material. USE - Preparation of composite material used for photocatalytic degradation of organic compound, and photocatalytic cracking of water for producing hydrogen. ADVANTAGE - The nano silver/graphene/P25 composite material is economically manufactured under mild conditions by simple process. DETAILED DESCRIPTION - Preparation of nano silver/graphene/P25 composite material involves adding graphene oxide into a mixed solution of water and organic solvent, and ultrasonically dispersing to obtain brown transparent and uniform dispersion (A) with concentration of 0.2-0.25 mg/mL, adding silver nitrate aqueous solution into the dispersion (A), and magnetically stirring the mixture to obtain nano silver/graphene oxide solution (B), then adding P25-type powder into solution (B), continuously stirring, refluxing and reacting obtained nano silver/graphene oxide/P25 aqueous/organic solvent solution at 100-150 degrees C for 10 hours in an oil bath, cooling the reaction mixture to room temperature, filtering, washing, and vacuum-drying obtained material. The mass ratio of silver nitrate, graphene oxide, and P25-type powder is 0.3:1:20-2:1:400.