• 专利标题:   Preparation of conductive diatomite-graphene composite for building material, involves adding peroxide solution into graphene solution, stirring, drying and obtaining graphene-coated powder, and mixing powder with ground diatomite.
  • 专利号:   CN104167258-A, CN104167258-B
  • 发明人:   GAO X, LI M, LI Y, ZHAO Z
  • 专利权人:   UNIV HARBIN ENGINEERING
  • 国际专利分类:   H01B001/18, H01B013/00
  • 专利详细信息:   CN104167258-A 26 Nov 2014 H01B-013/00 201507 Pages: 8 Chinese
  • 申请详细信息:   CN104167258-A CN10246846 05 Jun 2014
  • 优先权号:   CN10246846

▎ 摘  要

NOVELTY - Graphene is added to deionized water and ultrasonically-dispersed to obtain aqueous solution of graphene. A peroxide solution is poured into graphene solution, mechanically-stirred, and dried, to obtain graphene-coated powder. The obtained powder is mixed with ground diatomite, molded, pressed, heated and air-cooled to room temperature, to obtain conductive diatomite-graphene composite. USE - Preparation of conductive diatomite-graphene composite used for building material. ADVANTAGE - The method efficiently and economically provides environmentally-friendly conductive diatomite-graphene composite using simple process. DETAILED DESCRIPTION - Diatomite ore is sintered at 650 degrees C for 1 hour, and crushed to size of 20 mu m less. Graphene is added to deionized water and ultrasonically-dispersed for 5 hours, to obtain 0.1-1 mg/l aqueous solution of graphene. A peroxide solution is poured into the graphene solution, mechanically-stirred at 80 degrees C until obtaining sticky paste, and dried at 60 degrees C for 24 hours, to obtain graphene-coated powder. The obtained powder is mixed with diatomite, molded, pressed at room temperature in a vacuum furnace at pressure of 1x 104 Pa, heated to 850-870 degrees C at rate of 200 degrees C/hour or less, and air-cooled to room temperature when the temperature drops to 100 degrees C, to obtain conductive diatomite-graphene composite.