• 专利标题:   Preparation of poly(3,4-ethylenedioxythiophene)-doped beta-akaganeite/reduced graphene oxide array lithium ion battery anode material involves mixing iron salt and 3,4-ethylenedioxythiophene, dispersing with iron salt and graphene oxide.
  • 专利号:   CN108288700-A
  • 发明人:   CAO L, MA M, QI H, LI J, HUANG J, YAO K, CHEN W, WU G
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/52, H01M004/62
  • 专利详细信息:   CN108288700-A 17 Jul 2018 H01M-004/36 201855 Pages: 8 Chinese
  • 申请详细信息:   CN108288700-A CN10074265 25 Jan 2018
  • 优先权号:   CN10074265

▎ 摘  要

NOVELTY - Preparation of poly(3,4-ethylenedioxythiophene)-doped beta -akaganeite/reduced graphene oxide array lithium ion battery anode material comprises dissolving graphene oxide in 25-50 mL deionized water and ultrasonically dispersing; dropwise adding analytically pure soluble iron salt and 0.01-0.05 mL 3,4-ethylenedioxythiophene while stirring, dissolving, and ultrasonically dispersing with 0.05-0.5 mol/L iron salt and graphene oxide to obtain suspension; hydrothermal reacting at 50-150 degrees C and naturally cooling to room temperature; washing with water and alcohol and dispersing in water; and vacuum freeze-drying at - 20 degrees C to - 50 degrees C and 10-60 Pa. USE - Method for preparing poly(3,4-ethylenedioxythiophene)-doped beta -akaganeite/reduced graphene oxide array lithium ion battery anode material. ADVANTAGE - The lithium ion battery anode material has good reduction-oxidation property, good conductivity, large specific surface area, and improved dispersion of iron oxide, self-assembly morphology, and improved electrochemical performance.