• 专利标题:   Preparing boron-doped graphene or titanium dioxide nano-rods photocatalytic material, comprises e.g. ultrasonically dispersing graphene oxide in deionized water, stirring, performing hydro-thermal reaction, and performing vacuum drying.
  • 专利号:   CN103949234-A, CN103949234-B
  • 发明人:   LIU B, LI H, WANG Y, WU Q, WU B
  • 专利权人:   SHANGHAI RONGFU NEW MATERIALS CO LTD
  • 国际专利分类:   B01D053/56, B01D053/90, B01J021/18, B82Y030/00, B82Y040/00
  • 专利详细信息:   CN103949234-A 30 Jul 2014 B01J-021/18 201468 Pages: 13 Chinese
  • 申请详细信息:   CN103949234-A CN10165011 23 Apr 2014
  • 优先权号:   CN10165011

▎ 摘  要

NOVELTY - Preparing boron-doped graphene/titanium dioxide nano-rods photocatalytic material, comprises (i) producing graphene oxide by American Chemical society nano journal 2010 volume 4, pages 4806-4814; (ii) ultrasonically dispersing 8-80 mg graphene oxide in 15-25 ml deionized water, to obtain graphene oxide dispersion liquid; (iii) adding sodium borohydride and titanium trichloride solution into the graphite oxide dispersion liquid, and stirring under hydro-thermal reaction to obtain a precipitate; and (iv) washing, performing vacuum drying, grinding into a homogeneous powder. USE - The method is useful for preparing boron-doped graphene or titanium dioxide nano-rods photocatalytic material (claimed). ADVANTAGE - The method improves the photocatalytic activity of the composite material; and facilitates the chemical absorption of nitric oxide and nitrogen dioxide and other harmful gases, and the absorption and decomposition of harmful gases on the graphene surface. DETAILED DESCRIPTION - Preparing boron-doped graphene/titanium dioxide nano-rods photocatalytic material, comprises (i) producing graphene oxide based on the process mentioned in American Chemical society nano journal 2010 volume 4, pages 4806-4814; (ii) ultrasonically dispersing 8-80 mg graphene oxide in 15-25 ml deionized water, to obtain graphene oxide dispersion liquid; (iii) adding sodium borohydride and titanium trichloride solution into the graphite oxide dispersion liquid, and stirring while performing hydro-thermal reaction to obtain a precipitate; and (iv) washing the precipitate, carrying out vacuum drying, grinding into a homogeneous powder, to obtain the product, where graphene oxide, boron hydride and titanium trichloride are used as precursor.