▎ 摘　　要

NOVELTY - Synthesis of nano graphene structure compound comprises adding palladium acetate into sealing pipe, mixing triphosphorus (p-flouro-benzyne) (P (p-F-C6H4) 3), cesium pivalate (CsOPiv,) cesium carbonate (Cs2CO3) and solvent in glove box, stirring, adding o-aryl iodobenzene and bromonaphthol into sealing pipe, taking out sealing pipe from glove box, reacting, recovering reaction liquid to room temperature, using dichloromethane and saturated ammonium chloride solution to extract, extracting for three times and collecting organic phase. drying organic phase by drying agent, filtering, drying, and separating by column chromatography to obtain white solid product; and adding cerium chloride heptahydrate into white solid product, injecting inert gas to protect, injecting dried methanol into product, stirring, adding sodium borohydride. adding p-toluenesulfonic acid hydrate, quenching reaction, adding ethyl acetate, extracting, collecting organic phase, drying, filtering and separating. USE - The method is used for synthesizing nano graphene structure compound used in fluorescence, organic semiconductor material, luminescent material, solar cell, and photodiode. ADVANTAGE - The synthesis method is simple. The raw material is simple and easy to obtain. It has good stability in expanding production process. DETAILED DESCRIPTION - Synthesis of nano graphene structure compound comprises adding palladium acetate into sealing pipe, mixing triphosphorus (p-flouro-benzyne) (P (p-F-C6H4) 3), cesium pivalate (CsOPiv,) cesium carbonate (Cs2CO3) and solvent in glove box, stirring, adding o-aryl iodobenzene and bromonaphthol into sealing pipe, taking out sealing pipe from glove box, continuously reacting at high temperature, finishing reaction, recovering reaction liquid to room temperature, using dichloromethane and saturated ammonium chloride solution to extract, extracting for three times and collecting organic phase. drying organic phase by drying agent, filtering, drying, and separating by column chromatography to obtain white solid product; and adding cerium chloride heptahydrate into white solid product obtained in firts step, injecting inert gas to protect, injecting dried methanol into product, stirring at room temperature, adding sodium borohydride to reaction solution. adding p-toluenesulfonic acid hydrate into reaction liquid to react, quenching reaction, adding ethyl acetate into reaction liquid, extracting for 3 times, collecting organic phase, drying by drying agent, filtering, drying and separating by column chromatography.