• 专利标题:   Grafting terminal amino hyper-branched polymer with graphene oxide modified epoxy resin, by adding water and distilled water to graphite oxide, adding triethylene tetramine, and slowly adding methanol to reacting solution.
  • 专利号:   CN102504147-A, CN102504147-B
  • 发明人:   GUO D, LEE S, LIU K, LU S, LUO C, XU X
  • 专利权人:   UNIV GUILIN TECHNOLOGY
  • 国际专利分类:   C08F220/14, C08F292/00, C08L051/10, C08L063/00
  • 专利详细信息:   CN102504147-A 20 Jun 2012 C08F-292/00 201260 Pages: 6 Chinese
  • 申请详细信息:   CN102504147-A CN10391068 29 Nov 2011
  • 优先权号:   CN10391068

▎ 摘  要

NOVELTY - Grafting terminal amino hyper-branched polymer with graphene oxide modified epoxy resin, involves (a) adding (in ml): water (0-250) and distilled water (50-200) to graphite oxide and stirring for 10-50 minutes, (b) adding triethylene tetramine (5-25) to conical flask and adding N,N-dimethyl formamide to the conical flask, (c) slowly adding methanol (1-10) to the reacting solution, raising the temperature to 80-120 degrees C and reacting the solution for 6-10 hours, and (d) adding the solution obtained in step (a) to the reacting solution obtained in step (c). USE - The method is useful for grafting terminal amino hyper-branched polymer with graphene oxide modified epoxy resin. ADVANTAGE - The method is simple, environmentally-friendly, cost-effective, and suitable for industrialization. DETAILED DESCRIPTION - Method for grafting terminal amino hyper-branched polymer with graphene oxide modified epoxy resin, involves (a) adding (in ml): water (0-250) and distilled water (50-200) to graphite oxide and stirring for 10-50 minutes, (b) adding triethylene tetramine (5-25) to conical flask and adding N,N-dimethyl formamide to the conical flask and raising the temperature of the reacting solution to 55-65 degrees C, (c) slowly adding methanol (1-10) to the reacting solution, raising the temperature to 80-120 degrees C and reacting the solution for 6-10 hours, and (d) adding the solution obtained in step (a) to the reacting solution obtained in step (c).