• 专利标题:   Rapid preparation of graphene/silver sulfide quantum dot nanocomposites involves adding graphene oxide to silver nitrate, dispersing mixture in dimethyl sulfoxide solution, reacting mixture and then centrifuging, and drying.
  • 专利号:   CN104465127-A
  • 发明人:   LIU J, LI Z, OU B
  • 专利权人:   UNIV HUNAN SCI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, H01G011/24, H01G011/30, H01G011/86
  • 专利详细信息:   CN104465127-A 25 Mar 2015 H01G-011/86 201539 Pages: 9 Chinese
  • 申请详细信息:   CN104465127-A CN10672172 22 Nov 2014
  • 优先权号:   CN10672172

▎ 摘  要

NOVELTY - The method for rapid preparation of graphene/silver sulfide quantum dot nanocomposites involves adding graphene oxide to silver nitrate, uniformly mixing, dispersing the mixture in dimethyl sulfoxide solution to obtain a solution (A), adding graphene oxide to the solution (A) and then ultrasonically peeling, centrifuging the mixture and then separating, transferring the mixture to an autoclave and then reacting at 150-200 degrees C for 10-15 hours, washing the mixture using acetone and ethanol and distilled water, centrifuging the mixture, and drying under vacuum. USE - The method is useful for rapid preparation of graphene/silver sulfide quantum dot nanocomposites (claimed). ADVANTAGE - The energy-saving method enables rapid and simple preparation of graphene/silver sulfide quantum dot nanocomposites with high yield, and excellent stability and optoelectronic properties. DETAILED DESCRIPTION - The method for rapid preparation of graphene/silver sulfide quantum dot nanocomposites involves adding graphene oxide to silver nitrate in a mass ratio of 1:1-2, uniformly mixing, dispersing the mixture in dimethyl sulfoxide solution to obtain a solution (A), adding graphene oxide to the solution (A) and then ultrasonically peeling, centrifuging the mixture and then separating, transferring the mixture to an autoclave and then reacting at 150-200 degrees C for 10-15 hours, washing the mixture using acetone, ethanol and distilled water and then ultrasonically cleaning, centrifuging the mixture, and drying under vacuum. An INDEPENDENT CLAIM is included for graphene/silver sulfide quantum dot nanocomposites prepared by the method.