▎ 摘　　要

NOVELTY - Preparing macroscopic threedimensional 1 T- molybdenum disulphide (MoS2)/titanium dioxide (TiO2)/ graphene dioxide (rGO) composite photocatalytic material for photo-catalysis comprises (1) dispersing titanium source in hydrofluoric acid solution, using hydrothermal method to synthesize sheet with titanium dioxide characteristics of the sheet, (2) titanium dioxide the nano sheet into the mixed solution containing molybdenum and sulfur source, dispersing, in-situ growing metal phase molybdenum disulfide on the titanium dioxide of the sheet nano sheet by hydrothermal method, washing, the solid after drying is binary composite material 1 TMoS2/TiO2, (3) dispersing the binary composite material 1 T-MoS2/TiO2 in the graphene oxide aqueous solution, transferring to the high pressure reaction kettle for hydro-thermal processing to obtain the macroscopic three-dimensional 1 TMoS2/TiO2/rGO hydrogel, (4) circulating dialysis after freezing and drying. USE - The method is useful for preparing macroscopic three dimensional 1 T- molybdenum disulphide/titanium dioxide/ graphene dioxide composite photocatalytic material for photo-catalysis.