• 专利标题:   Preparing gold-magnetite/graphene/titanium dioxide photocatalyst comprises adding ferrous sulfate and ferric sulfate in deionized water, stirring and then adding aqueous ammonia, and ultrasonically vibrating precipitate.
  • 专利号:   CN103285879-A
  • 发明人:   MA Y
  • 专利权人:   MA Y
  • 国际专利分类:   B01J023/89
  • 专利详细信息:   CN103285879-A 11 Sep 2013 B01J-023/89 201382 Pages: 5 Chinese
  • 申请详细信息:   CN103285879-A CN10188669 16 May 2013
  • 优先权号:   CN10188669

▎ 摘  要

NOVELTY - Preparing gold-magnetite/graphene/titanium dioxide photocatalyst comprises adding ferrous sulfate and ferric sulfate in deionized water, stirring and dissolving the mixture by nitrogen as protective gas, adding aqueous ammonia to obtain black precipitate, continuously stirring and ultrasonically vibrating the precipitate to obtain magnetite nano suspension, adding proper amount of chloroform solution in the suspension, mixing hydrogen tetrachloroaurate(III) hydrate, oleylamine and tertiary butyl amine borane, stirring the mixture to obtain gold-modified magnetite nanoparticles. USE - The method is useful for preparing gold-magnetite/graphene/titanium dioxide photocatalyst (claimed). DETAILED DESCRIPTION - Preparing gold-magnetite/titanium dioxide photocatalyst comprises adding ferrous sulfate and ferric sulfate in deionized water, stirring and dissolving the mixture by nitrogen as protective gas at 40-60 degrees C, adding aqueous ammonia to obtain black precipitate, continuously stirring and ultrasonically vibrating the precipitate to obtain magnetite nano suspension, adding proper amount of chloroform solution in the suspension, mixing hydrogen tetrachloroaurate(III) hydrate, oleylamine and tertiary butyl amine borane, stirring the mixture for 20 minutes to obtain gold-modified magnetite nanoparticles, preparing graphene/titanium mixed solution by sol-gel method, and adding hydrothermal gold-modified magnetite nanoparticles in the graphene/titanium mixed solution and then stirring.