• 专利标题:   Preparing graphene-nano silver for low-temperature conductive silver paste, comprises e.g. preparing graphene dispersion liquid; preparing silver solution system containing graphene; and adjusting PH value of silver solution system.
  • 专利号:   CN111292871-A
  • 发明人:   MA J, LIU F
  • 专利权人:   CHANGSHA NEW MATERIAL IND RES INST CO LT
  • 国际专利分类:   B22F009/24, B33Y030/00, B82Y040/00, H01B001/22
  • 专利详细信息:   CN111292871-A 16 Jun 2020 H01B-001/22 202058 Pages: 10 Chinese
  • 申请详细信息:   CN111292871-A CN11377619 27 Dec 2019
  • 优先权号:   CN11377619

▎ 摘  要

NOVELTY - Preparing graphene-nano silver for low-temperature conductive silver paste, comprises (1) preparing graphene dispersion liquid; (2) preparing silver solution system containing graphene; and (3) adjusting the PH value of the silver solution system containing graphene and dispersant, and dropping a reducing agent at the first reaction temperature to reduce the nano silver particles; where in the step (1), the graphene dispersion liquid is 0.2-0.4 mg/ml graphene dispersion liquid; in the step (1), the graphene is not graphene oxide; in the step (2), dispersant in the silver solution containing graphene is polyvinylpyrrolidone, and solvent is nitromethylpyrrolidone. USE - The method is useful for preparing graphene-nano silver for low-temperature conductive silver paste. ADVANTAGE - The nano silver: has particle size of 10-500 nm; and can reduces the resistivity of conductive silver paste. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for the graphene-nano silver material is prepared by above mentioned method.