• 专利标题:   Preparing graphene comprises mixing organic solvent with graphite powder, stirring mixture, quickly raising the temperature and then maintaining the temperature for specific period, and cooling mixture and then centrifuging.
  • 专利号:   CN103922325-A, CN103922325-B
  • 发明人:   LIU J, LIU L, LIU Q, WANG J, YAN Y, YU L, GAO Z, YANG W
  • 专利权人:   UNIV HARBIN ENGINEERING
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103922325-A 16 Jul 2014 C01B-031/04 201467 Pages: 6 Chinese
  • 申请详细信息:   CN103922325-A CN10153109 17 Apr 2014
  • 优先权号:   CN10153109

▎ 摘  要

NOVELTY - Preparing graphene comprises: mixing an organic solvent with a graphite powder according to mass ratio of 100-10000:1, stirring the mixture for 0.5-2 hours at -30 degrees C to 0 degrees C, quickly raising the temperature to 100-200?C, and maintaining the temperature for 0.5-4 hours; cooling the mixture, and centrifuging the cooled mixture to obtain a graphene-containing liquid; continuously adding the organic solvent with the liquid, repeating the above steps until a solid residue is disappeared; and filtering the graphene-containing liquid and then washing using ethanol, and drying the washed liquid. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The method is capable of preparing the graphene in a simple and cost-effective manner with simple structure, less pollution and high quality. DETAILED DESCRIPTION - Preparing graphene comprises: mixing an organic solvent with a graphite powder according to mass ratio of 100-10000:1, stirring the mixture for 0.5-2 hours at -30 degrees C to 0 degrees C, quickly raising the temperature to 100-200?C, and maintaining the temperature for 0.5-4 hours; cooling the mixture, and centrifuging the cooled mixture to obtain a graphene-containing liquid; continuously adding the organic solvent with the liquid, repeating the above steps until a solid residue is disappeared; and filtering the graphene-containing liquid and then washing using ethanol, and drying the washed liquid at 80 degrees C for 12 hours.