• 专利标题:   Preparing graphene two-dimensional nano-sheet comprises adding stripped layered material into anhydrous solvent, stirring, adding alkali metal into dispersion, dispersing, washing the crude product, treating ultrasonically and washing.
  • 专利号:   CN104402053-A, CN104402053-B
  • 发明人:   FENG H, HU Z, LIU X
  • 专利权人:   UNIV CHINESE ACAD SCI
  • 国际专利分类:   B82Y030/00, C01B021/064, C01G039/06, C01G041/00
  • 专利详细信息:   CN104402053-A 11 Mar 2015 C01G-039/06 201532 Pages: 11 Chinese
  • 申请详细信息:   CN104402053-A CN10612347 04 Nov 2014
  • 优先权号:   CN10612347

▎ 摘  要

NOVELTY - Preparing graphene two-dimensional nano-sheet comprises: (i) adding 1 g stripped layered material into each 100-1000 ml anhydrous solvent and stirring to disperse; (ii) adding an alkali metal into the resultant dispersion (1 g alkali metal accounts for 0.25-5 g layered material), then dispersing at 10-80 degrees C by stirring or shearing at 200-20000 rotations/minute for 6-120 hours to obtain a crude product; and (iii) washing the crude product with anhydrous solvent for 3-5 times, dispersing the product in water, treating ultrasonically for 5-60 minutes, washing the product with water to pH 6-8. USE - The method is useful for preparing graphene two-dimensional nano-sheet (claimed). ADVANTAGE - The nano-sheet is simple and economical to prepare, produces high yield and suitable for large scale production.