• 专利标题:   Production of carbon nanotubes for preparing graphene nanoribbons, involves subjecting metal substrate to acid treatment, heating substrate, ultrasonically treating, and processing substrate in chemical vapor deposition reactor.
  • 专利号:   CN103935976-A, CN103935976-B
  • 发明人:   WANG Y, WU F, YUAN X, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING ENG CO LTD, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   B82Y030/00, C01B031/02, C01B031/04
  • 专利详细信息:   CN103935976-A 23 Jul 2014 C01B-031/02 201468 Pages: 13 Chinese
  • 申请详细信息:   CN103935976-A CN10019518 18 Jan 2013
  • 优先权号:   CN10019518

▎ 摘  要

NOVELTY - Production of carbon nanotubes involves subjecting a metal substrate to acid treatment in an oxygen-free environment, heating substrate at 600-900 degrees C, ultrasonically treating, placing substrate in chemical vapor deposition reactor containing gaseous carbonaceous material, supplying protective gas to the reactor and removing carbon nanotubes from the substrate. USE - Production of carbon nanotubes used for preparing graphene nanoribbons (all claimed). ADVANTAGE - The method efficiently and economically provides carbon nanotubes with high thickness and shape uniformity, using simple process under controlled reaction conditions. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) carbon nanotubes; (2) preparation of graphene nanoribbons, which involves mixing carbon nanotubes and metal chloride in mass ratio of 1:0.8-1:1.2 at 460-550 degrees C and obtaining metal chloride intercalated carbon nanotubes, mixing metal chloride intercalated carbon nanotubes and acetone in mass ratio of 1 g:100-1000 mL, ultrasonically peeling after separation and purifying; and (3) graphene nanoribbons.