• 专利标题:   Graphene solution preparation involves mixing graphite powder and hydrogen peroxide, and processing using cobalt-60 to obtain graphene suspension.
  • 专利号:   CN103011153-A, CN103011153-B
  • 发明人:   ZENG X, CHEN H, XIA Z, ZHU P, ZENG Y, WANG L, WANG H, HOU Y, HUANG X, ZHAO G
  • 专利权人:   SICHUAN LANYUE TECHNOLOGY CO LTD, INST BIOTECHNOLOGY NUCLEAR TECHNOLOGY, INST BIOTECHNOLOGY NUCLEAR TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103011153-A 03 Apr 2013 C01B-031/04 201366 Pages: 8 Chinese
  • 申请详细信息:   CN103011153-A CN10026685 24 Jan 2013
  • 优先权号:   CN10026685

▎ 摘  要

NOVELTY - A graphene solution is prepared by mixing graphite powder and hydrogen peroxide at a mass ratio of 1:2-5; placing cobalt-60 into chamber to produce gamma -rays with intensity of 0.03-0.1 KGY, 0.2-2.5 KGY, and 0.01-0.03 KGY, respectively for 1-2 hours, 2-4 hours and 1-2 hours to obtain graphene suspension; adding the graphene suspension with formaldehyde, ethanol, phenol, aniline, or diethylenetriamine at a mass ratio of 3:1; processing the mixture with cobalt-60 for 0 5-1 hour, reacting at 10-250 kHz ultrasonic oscillating action for 2 hours, and obtaining product. USE - Method for preparation of graphene solution (claimed). ADVANTAGE - The method is simple to operate, safe and clean, and suitable for large-scale production.