• 专利标题:   Method for preparing graphene-carbon nano-tube composite material useful as conductive additive in lithium ion battery comprises adding graphene oxide material completely oxidized into diluted acid solution, and performing acid washing operations.
  • 专利号:   CN113428851-A, CN113428851-B
  • 发明人:   ZHENG T, ZHANG M, MAO O, YE Z, CHENG L, XU H
  • 专利权人:   JIANGSU CNANO TECHNOLOGY CO LTD
  • 国际专利分类:   H01M004/62, C01B032/194, C01B032/174, C01B032/168, C01B032/17, C01B032/184
  • 专利详细信息:   CN113428851-A 24 Sep 2021 C01B-032/184 202104 Chinese
  • 申请详细信息:   CN113428851-A CN10655600 11 Jun 2021
  • 优先权号:   CN10655600

▎ 摘  要

NOVELTY - The method comprises adding graphene oxide material completely oxidized into a diluted acid solution, and stirring uniformly to obtain a component, adding carbon nano-tube powder into component, stirring uniformly, filtering, and taking filter residue to obtain graphene oxide/carbon nano-tube filter material, adding filter material of graphene oxide and carbon nano-tube filter material into dilute acid solution and stirring evenly, completing first acid washing operation, repeating acid washing operations for at least three times, extruding, granulating, drying and thermal reduction to obtain final product. USE - The method is useful for preparing graphene-carbon nano-tube composite material, which is useful as conductive additive in lithium ion battery. ADVANTAGE - The material: is environmentally friendly; has good conductivity; reduces acid purification process and waste liquid amount, acid cleaning cost, good dispersion uniformity and conductive balance problem. The method: improves conductivity of electrode material, and mechanical performance of composite material. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: (1) graphene-carbon nano-tube composite material; (2) graphene-carbon nano-tube composite slurry; and (3) preparing graphene-carbon nano-tube composite slurry.