• 专利标题:   Preparation of graded porous structure foam metal involves washing foam metal, drying, soaking in N-methylpyrrolidone-containing polyaniline, drying, preparing enriched graphene solution using improved Hummer method, and ultrasonic treating.
  • 专利号:   CN107119248-A
  • 发明人:   ZHAO J, CHEN L, LIU X, LI Y
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   C22F001/02, C22F001/08, C22F001/10, H01M004/38
  • 专利详细信息:   CN107119248-A 01 Sep 2017 C22F-001/10 201768 Pages: 21 Chinese
  • 申请详细信息:   CN107119248-A CN10368947 23 May 2017
  • 优先权号:   CN10368947

▎ 摘  要

NOVELTY - Preparation of graded porous structure foam metal involves washing foam metal, drying, soaking in N-methylpyrrolidone-containing polyaniline for 2-10 hours, drying, preparing enriched graphene solution using improved Hummer method, ultrasonic treating graphene and polystyrene ball solution for 20-60 minutes, mixing at mass ratio of 1:10-40, stirring for 10-30 minutes, ultrasonic treating for 10-30 minutes, soaking foamed metal for 2-10 hours, heating at 50-80 degrees C, drying, placing in corundum porcelain boat, annealing under ammonia-argon mixed gas, and heating at 700-1000 degrees C for 1-4 hours. USE - Method for preparing graded porous structure foam metal. DETAILED DESCRIPTION - Preparation of graded porous structure foam metal comprises washing foam metal, drying, soaking in N-methylpyrrolidone-containing polyaniline for 2-10 hours, drying, preparing enriched graphene solution using improved Hummer method, ultrasonic treating graphene and polystyrene ball solution for 20-60 minutes, mixing at mass ratio of 1:10-40, stirring for 10-30 minutes, ultrasonic treating for 10-30 minutes, soaking foamed metal for 2-10 hours, heating at 50-80 degrees C, drying, placing in corundum porcelain boat, annealing under ammonia-argon mixed gas, heating at 700-1000 degrees C for 1-4 hours, cooling to 100-500 degrees C, and cooling to room temperature.