• 专利标题:   Preparation of graphene composite material involves dispersing nitrogen-doped titanium dioxide powder in water to form suspension, adding graphene oxide solution, reacting, cooling, centrifuging, washing with distilled water, and drying.
  • 专利号:   CN116173996-A
  • 发明人:   GUO H, WENG X
  • 专利权人:   UNIV LIAONING TECHNOLOGY
  • 国际专利分类:   B01J027/24, C01G023/047, C02F001/30, C02F101/30
  • 专利详细信息:   CN116173996-A 30 May 2023 B01J-027/24 202353 Chinese
  • 申请详细信息:   CN116173996-A CN11419213 26 Nov 2021
  • 优先权号:   CN11419213

▎ 摘  要

NOVELTY - Preparation of graphene composite material involves (s1) ultrasonically dispersing 0.2 g nitrogen-doped titanium dioxide powder in water for 20 minutes to form a suspension, (s2) adding a graphene oxide solution into the suspension and ultrasonically processing for 30 minutes to uniformly disperse the graphene oxide solution, and (s3) adding the obtained liquid into a reaction vessel, continuously stirring and reacting for 6 hours in an oil bath at 160℃, naturally cooling to room temperature, centrifuging and separating the prepared product, washing with distilled water, and drying in a blast drying oven for 5 hours at 80℃ to obtain nitrogen-doped titanium dioxide-graphene composite material. The composite material comprises nitrogen-doped titanium dioxide powder, graphene, surfactant, graphene oxide solution, anhydrous ethanol and water. USE - Preparation of graphene composite material. ADVANTAGE - The method uses nitrogen doping of titanium dioxide powder to reduce forbidden band width and make the titanium dioxide have visible light activity without reducing UV light activity.