• 专利标题:   Preparing functionalized graphene oxide-hypophosphite flame retardant used in preparing polystyrene nano-composite flame retardant material, involves preparing phosphorus-containing functionalized graphene oxide.
  • 专利号:   CN113121882-A, CN113121882-B
  • 发明人:   DENG Z, DAI K, LIU G, WU Y, ZHAO C
  • 专利权人:   UNIV GUANGDONG TECHNOLOGY
  • 国际专利分类:   C08K003/04, C08K003/32, C08K009/02, C08K009/04, C08L025/06
  • 专利详细信息:   CN113121882-A 16 Jul 2021 C08K-009/04 202176 Pages: 11 Chinese
  • 申请详细信息:   CN113121882-A CN10249677 08 Mar 2021
  • 优先权号:   CN10249677

▎ 摘  要

NOVELTY - Preparing functionalized graphene oxide-hypophosphite flame retardant involves preparing phosphorus-containing functionalized graphene oxide by mixing the graphene oxide, phosphorus oxychloride, triethylamine in dimethylformamide solution uniformly, under the inert gas atmosphere, reacting for 5-8 hours at 0-5 degrees C to obtain the mixed solution, mixing the DOPO-OH with the mixed solution uniformly, reacting for 5-8 hours at 40-60 degrees C, post-processing to obtain phosphorus-containing functionalized graphene oxide, preparing functionalized graphene oxide-hypophosphite flame retardant by mixing the sodium hypophosphite with aqueous solution of phosphorus-containing functionalized graphene oxide uniformly, adding octahydrate aluminum sulfate aqueous solution dropwise at 80-90 degrees C, reacting for 6-8 hours, post-processing to obtain the functionalized graphene oxide-hypophosphite flame retardant. USE - Method for preparing functionalized graphene oxide-hypophosphite flame retardant used in preparing polystyrene nano-composite flame retardant material (claimed). ADVANTAGE - The method has excellent flame-retardant effect. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing polystyrene nano-composite flame retardant material, which involves: (A) dispersing the functionalized graphene oxide-hypophosphite flame retardant and polystyrene in dimethylformamide solution, mixing uniformly, drying, granulating to obtain polystyrene nano-material masterbatch; and (B) mixing the polystyrene nano-material master batch and polystyrene, obtaining polystyrene nano-composite flame retardant material.