• 专利标题:   Preparation of flame-retardant material with multi-layer structure, involves mixing graphene oxide and N,N-dimethylformamide, adding intumescent flame retardant, then adding dicyclohexylcarbodiimide, centrifuging, and injection molding.
  • 专利号:   CN112940463-A
  • 发明人:   LI Z, CHEN B, WANG Z, ZHAO T, LIAO L, LI J
  • 专利权人:   UNIV XIHUA
  • 国际专利分类:   C08K003/04, C08K005/29, C08L067/02, C08L091/06
  • 专利详细信息:   CN112940463-A 11 Jun 2021 C08L-067/02 202164 Pages: 17 Chinese
  • 申请详细信息:   CN112940463-A CN10122592 29 Jan 2021
  • 优先权号:   CN10122592

▎ 摘  要

NOVELTY - A preparation of flame-retardant material, involves (1) mixing graphene oxide and N,N-dimethylformamide, ultrasonically shaking at 30-50 degrees C for 20-40 minutes, and then adding intumescent flame retardant, ultrasonically oscillating for 20-40 minutes at the temperature of 30-50 degrees C, then adding dicyclohexylcarbodiimide, mechanically stirring for 15-25 hours in a water bath at 40-60 degrees C, and finally centrifuging, cleaning and drying in sequence to obtain the modified flame retardant, (2) drying the intumescent flame retardant and polybutylene terephthalate at a temperature of 70-90 degrees C for 8-12 hours, and then mixing them according to different mass ratios to obtain a mixture, adding the modified flame retardant obtained in step (1), and pelletizing by a co-rotating twin-screw extruder, drying and injection molding. USE - Preparation of flame-retardant material with multi-layer structure (claimed). ADVANTAGE - The flame retardant material combines a concentration gradient layered structure and a layered structure, maintains the mechanical properties, but also improves the flame-retardant properties. The flame retardant material effectively solves the problems of reduced mechanical properties and higher cost after the addition of flame retardants.