• 专利标题:   Preparing supported porous nano platinum catalyst in hydrogenation of toluene to prepare cyclohexane, involves adding platinum precursor, template agent, and reducing agent to deionized water, stirring, centrifuging, washing, and drying.
  • 专利号:   CN112973676-A
  • 发明人:   YANG Y, HUANG J, LIU C
  • 专利权人:   CAS DALIAN CHEM PHYSICAL INST
  • 国际专利分类:   B01J023/42, B01J023/63, B01J023/89, B01J035/00, C07C013/18, C07C209/48, C07C211/27, C07C005/10
  • 专利详细信息:   CN112973676-A 18 Jun 2021 B01J-023/42 202168 Pages: 10 Chinese
  • 申请详细信息:   CN112973676-A CN11295722 16 Dec 2019
  • 优先权号:   CN11295722

▎ 摘  要

NOVELTY - Preparing supported porous nano platinum catalyst involves adding platinum precursor, template agent, and reducing agent to deionized water, stirring at 25-50 degrees C or ultrasonic for 1-24 hours, centrifuging, washing, and drying to obtain porous nano-platinum particles, where the molar ratio of the platinum precursor, template agent, and reducing agent is 1:10-200:1000-50,000, dispersing the porous nano platinum particles obtained in deionized water, stirring at 25-50 degrees C or ultrasonic for 10-120 minutes to disperse, then adding carrier, stirring for 2-24 hours, then centrifuging and drying. The mass ratio of the porous nano platinum particles to the carrier is 0.1-5.0%. The sample obtained after drying is calcined at 50-1000 degrees C in nitrigen or hydrogen or air atmosphere for 1-24 hours to obtain product. USE - Method for preparing supported porous nano platinum catalyst used in hydrogenation of toluene to prepare cyclohexane, or to the hydrogenation of terephthalonitrile to prepare p-xylylenediamine, or hydrogenation of isophthalonitrile to prepare metaxylylenediamine, or the hydrogenation of phthalonitrile to prepare o-xylylenediamine (claimed). ADVANTAGE - The method catalyzes hydrogenation reaction under mild reaction condition.