• 专利标题:   Preparing polyphenylenesulfide composite material grafted by reducing graphene oxide used in preparing anti-corrosion coating involves using anhydrous sodium sulfide, dichlorobenzene and 2,5-dichloroaniline as raw material, reacting, washing & ultrasonically dispersing graphene oxide and drying.
  • 专利号:   CN114933712-A
  • 发明人:   WANG B, WANG N, GUO W, GUO X, LIU N, MO Z, FANG M, GUO R
  • 专利权人:   UNIV NORTHWEST NORMAL
  • 国际专利分类:   C01B032/194, C08G083/00, C09D187/00, C09D005/08
  • 专利详细信息:   CN114933712-A 23 Aug 2022 C08G-083/00 202204 Chinese
  • 申请详细信息:   CN114933712-A CN10715099 23 Jun 2022
  • 优先权号:   CN10715099

▎ 摘  要

NOVELTY - Preparing polyphenylenesulfide composite material grafted with graphene oxide involves using anhydrous sodium sulfide, dichlorobenzene and dichloroaniline as raw material, N-methyl pyrrolidone as solvent, using isopropyl titanate as catalyst, using nitrogen as protective gas, reacting for 1.5 ~ 2.5 hr at 260 ~ 280 degrees centigrade in alkaline environment, washing the sample, filtering, drying to obtain amination polyphenylthioether and (ii) ultrasonically dispersing the graphene oxide in tetrahydrofuran solution, adding aminated polyphenylenesulfide, stirring and reacting for 10 ~ 12h at 45 ~ 55 degrees centigrade to obtain polyphenylenesulfide-graphene oxide, adding hydrazine hydrate, reacting for 1.5 ~ 2.5 h at 75 ~ 85 degrees centigrade washing and drying to obtain polyphenylenesulfide. USE - Polyphenylenesulfide composite material grafted by reducing graphene oxide used in preparing anti-corrosion coating