• 专利标题:   Preparing reduced graphene oxide-polyimide heat-treated foam involves taking rectangular polyimide foam and immersing in graphene oxide aqueous solution, performing vacuum infiltration method and evacuating bubbles inside polyimide foam.
  • 专利号:   CN107266912-A
  • 发明人:   LV X, YANG J, LI X
  • 专利权人:   UNIV XIDIAN
  • 国际专利分类:   C01B032/19, C08K003/04, C08K009/04, C08L079/08
  • 专利详细信息:   CN107266912-A 20 Oct 2017 C08L-079/08 201778 Pages: 12 Chinese
  • 申请详细信息:   CN107266912-A CN10476513 21 Jun 2017
  • 优先权号:   CN10476513

▎ 摘  要

NOVELTY - Preparing reduced graphene oxide-polyimide heat-treated foam involves taking rectangular polyimide foam having length size of 1x 1x 1x 0.5cm and immersing in graphene oxide aqueous solution with mass concentration of 1-4 mg/ml, performing vacuum infiltration method and evacuating the bubbles inside polyimide foam to make graphene oxide adhere to surface of polyimide foam to obtain graphene oxide-polyimide foam. USE - Method for preparing reduced graphene oxide-polyimide heat-treated foam (claimed). ADVANTAGE - The method enables to prepare reduced graphene oxide-polyimide heat-treated foam is cost effective, has good mechanical property, complex preparation process, large density, improves the conductivity, and increases pressure sensitivity. DETAILED DESCRIPTION - Preparing reduced graphene oxide-polyimide heat-treated foam involves taking rectangular polyimide foam having length size of 1x 1x 1x 0.5cm and immersing in graphene oxide aqueous solution with mass concentration of 1-4 mg/ml, performing vacuum infiltration method and evacuating the bubbles inside polyimide foam to make graphene oxide adhere to surface of polyimide foam to obtain graphene oxide-polyimide foam. The obtained graphene oxide-polyimide foam is immersed in aqueous solution of chemical reducing agent in mass ratio of 3-4:1, and then bubbles are evacuated and subjected to chemical reduction reaction, cleaned to obtain reduced graphene oxide-polyimide foam. The obtained reduced graphene oxide-polyimide foam is placed in tube furnace, under protective gas to thermal reduction to obtain final product.