• 专利标题:   Preparation of fatigue-resistant biomimetic graphene nanocomposite material involves adding specific buffer solution and dopamine solution to aqueous solution of enriched graphene, crosslinking, adding nickel chloride and assembling.
  • 专利号:   CN106832273-A, CN106832273-B
  • 发明人:   CHENG Q, WAN S, HU W
  • 专利权人:   UNIV BEIHANG, UNIV BEIHANG
  • 国际专利分类:   C08G073/06, C08K003/04, C08K003/16, C08K007/00
  • 专利详细信息:   CN106832273-A 13 Jun 2017 C08G-073/06 201761 Pages: 11 Chinese
  • 申请详细信息:   CN106832273-A CN11144293 13 Dec 2016
  • 优先权号:   CN11144293

▎ 摘  要

NOVELTY - Preparation of fatigue-resistant biomimetic graphene nanocomposite material involves preparing aqueous solution of enriched graphene by ultrasonic method, adding a tris-hydroxymethylaminomethane buffer solution and a dopamine solution, crosslinking to form an oxidized graphene-polydopamine heterogeneous primer, adding nickel chloride solution, crosslinking, forming chelated structure, assembling the solution into nanocomposite by vacuum filtration, reducing, washing, drying and repeating the processes. USE - Preparation of fatigue-resistant biomimetic graphene nanocomposite material (claimed). ADVANTAGE - The biomimetic graphene nanocomposite material having excellent fatigue resistance, conductivity, strength and toughness is manufactured. DETAILED DESCRIPTION - Preparation of fatigue-resistant biomimetic graphene nanocomposite material involves preparing aqueous solution of enriched graphene by ultrasonic method, adding a tris-hydroxymethylaminomethane buffer solution and a dopamine solution to the graphene solution under stirring, performing covalent crosslinking to form an oxidized graphene-polydopamine (GO-PDA) heterogeneous primer, adding nickel chloride solution in drops, crosslinking, forming chelated structure to obtain uniformly dispersed mixed solution, assembling the mixed solution into nanocomposite by vacuum filtration, reducing with hydroiodic acid, washing, drying to produce graphene nanocomposites material, producing hetero-based material with different polydopamine contents by regulating the volume of dopamine solution, determining the optimal value of the polydopamine, regulating content of graphene oxide and nickel ion, and repeating the processes.