• 专利标题:   Preparation of recyclable titanium dioxide (P25)/graphene/ternary iron oxide photocatalytic material involves dissolving ferric salt in ethylene glycol, adding titanium dioxide/graphene composite, mixing, adding ammonia and mixing.
  • 专利号:   CN104874398-A
  • 发明人:   CHENG L, DING G, JIAO Z, WANG R, ZHANG S
  • 专利权人:   UNIV SHANGHAI
  • 国际专利分类:   B01J023/745, C02F001/32, C02F101/38
  • 专利详细信息:   CN104874398-A 02 Sep 2015 B01J-023/745 201619 Pages: 10 Chinese
  • 申请详细信息:   CN104874398-A CN10274880 26 May 2015
  • 优先权号:   CN10274880

▎ 摘  要

NOVELTY - Preparation of recyclable titanium dioxide (P25)/graphene/ternary iron oxide photocatalytic material involves dissolving ferric salt in ethylene glycol, adding titanium dioxide (P25)/graphene binary composite material, placing the mixed solution in an ultrasonic oscillator and mixing, adding the resultant mixed solution into a sealed reactor, adding ammonia, mixing, washing, centrifuging and vacuum-drying obtained solid. USE - Preparation of recyclable titanium dioxide (P25)/graphene/ternary iron oxide photocatalytic material (claimed). ADVANTAGE - The method enables preparation of photocatalytic material having high photocatalytic efficiency, strong magnetism, stable performance and excellent recyclability. DETAILED DESCRIPTION - Preparation of recyclable titanium dioxide (P25)/graphene/ternary iron oxide photocatalytic material involves weighing 1-5 mg graphene oxide using electronic balance, uniformly mixing 30 mL ethanol and water in a volume ratio of 1:1-2:1, adding 0.8-1.4 g commercial titanium dioxide (P25) powder, stirring uniformly using magnetic stirrer for 1-2 hours, placing the mixed solution in a sealed reactor, reacting at 80-120 degrees C for 1-3 hours, hydrothermally washing using distilled water, centrifuging to remove unreacted material, vacuum-drying obtained solid at 60 degrees C for 6-8 hours in an oven to obtain titanium dioxide (P25)/graphene binary composite material, weighing 0.2-0.6 g ferric salt such as ferric nitrate or ferric chloride using electronic balance, dissolving the salt in 10-20 mL ethylene glycol, adding predetermined amount of titanium dioxide (P25)/graphene binary composite material, where the concentration ratio of titanium dioxide (P25)/graphene binary composite material and ironion is 0.5:1-2:1, placing the mixed solution in an ultrasonic oscillator and mixing for 1-3 hours, adding the resultant mixed solution into a sealed reactor, adding 5-15 mL ammonia, mixing at 120-1800 degrees C for 8-12 hours, washing with ethanol and distilled water, centrifuging to remove unreacted material and vacuum-drying obtained solid at 60-80 degrees C for 4-8 hours.