• 专利标题:   Electrosynthesizing graphene composite electrode comprises (1) placing graphene oxide, adding pyrrole, adding organic sulfonate hole-expanding dopant, stirring, immersing in a black nanosol through nitrogen, polymerizing and drying.
  • 专利号:   CN111115769-A
  • 发明人:   LIU Y, XU K, AN Z, LI Q, ZHAO H
  • 专利权人:   INST SEAWATER DESALINATION MULTIPURPOS
  • 国际专利分类:   C02F001/469
  • 专利详细信息:   CN111115769-A 08 May 2020 C02F-001/469 202044 Pages: 14 Chinese
  • 申请详细信息:   CN111115769-A CN11383718 27 Dec 2019
  • 优先权号:   CN11383718

▎ 摘  要

NOVELTY - Electrosynthesizing graphene composite electrode comprises (1) placing graphene oxide with an interface zeta potential of 20 to -35 mv in container, adding pyrrole, adding an organic sulfonate hole-expanding dopant, adjusting the pH to 2.5-4.5 with benzenesulfonic acid, remainder being water, ultrasound or stirring to obtain black nanosol, storing under nitrogen, where the final concentration of graphene oxide is 0.3-0.8 g/l, final concentration of pyrrole is 0.1-0.5 mol/l and final concentration of the agent is 0-40 g/l and (2) using a three-dimensional mesh-shaped conductive support frame as the working electrode, immersing in a black nanosol through nitrogen at a current density of 2-5 mA/cm2 and an electric quantity of 0.5-20 C/cm2, 20-40 degrees C, depositing black nanosol and polymerizing on the three-dimensional network conductive support framework, rinsing with distilled water to removing impurities and drying to make graphene composite electrode. USE - The method is useful for electrosynthesizing graphene composite electrode. ADVANTAGE - The electrode: has even distribution of components and easy storage; and is suitable for electroabsorption and desalination operations compared with conventional porous carbon electrode. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene composite electrode.