• 专利标题:   Method for wet preparation of graphene from glycerin as liquid phase in planetary ball mill path, involves setting mass of graphite to predetermined value and setting mol ratio of graphite to propanetriol to predetermined ratio.
  • 专利号:   CN107572512-A
  • 发明人:   MA Z, WANG Q, SONG P, YANG Z, ZHANG J, LU L
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN107572512-A 12 Jan 2018 C01B-032/19 201809 Pages: 6 Chinese
  • 申请详细信息:   CN107572512-A CN11003384 24 Oct 2017
  • 优先权号:   CN11003384

▎ 摘  要

NOVELTY - The method involves pouring the liquid in an agate tank at a certain temperature, maintaining the temperature, and shaking to uniform state. The planetary ball mill is connected to the agate tank, after a certain speed and a certain time. The liquid in the agate tank is mixed with de-ionized water after centrifuging. The freezing and drying of supernatant is carried out after a certain time to obtain graphene, in which the mass of graphite is 0.5-5 g, and the mol ratio of graphite to propanetriol is 1:2-7. USE - Method for wet preparation of graphene from glycerin as liquid phase in planetary ball mill path. ADVANTAGE - The process is carried out simply and at low cost, and the prepared graphene has low defect.