• 专利标题:   Preparation of conductive filler, involves adding graphene oxide, thiol-modified multi-walled carbon nanotube to alcohol, adding resorcinol and silver nanowire to obtained solution, reacting, freeze-drying obtained gel and heat treating.
  • 专利号:   CN107189103-A
  • 发明人:   GU Y
  • 专利权人:   GU Y
  • 国际专利分类:   C08K003/04, C08K007/06, C08K007/24, C08K009/04, C09J011/04, C09J163/00, C09J175/04, C09J009/02
  • 专利详细信息:   CN107189103-A 22 Sep 2017 C08K-009/04 201773 Pages: 8 Chinese
  • 申请详细信息:   CN107189103-A CN10513844 29 Jun 2017
  • 优先权号:   CN10513844

▎ 摘  要

NOVELTY - Preparation of conductive filler, involves modifying multi-walled carbon nanotube with thiol, adding graphene oxide and thiol-modified multi-walled carbon nanotube to hydroalcoholic solution, adding resorcinol, formaldehyde, sodium carbonate and silver nanowires to obtained solution under ultrasonic condition to obtain mixed solution, reacting mixed solution at 70-80 degrees C for 48-96 hours to obtain gel, freeze-drying obtained gel for 48-96 hours to obtain aerogel, carrying out heat treatment with aerogel at 200-400 degrees C and carrying out secondary heat treatment at 650-750 degrees C. USE - Preparation of conductive filler (claimed). ADVANTAGE - The method enables preparation of conductive filler with excellent conductivity. The three-dimensional conductive filler has excellent synergistic effect. DETAILED DESCRIPTION - Preparation of conductive filler, involves modifying multi-walled carbon nanotube with thiol, adding graphene oxide and thiol-modified multi-walled carbon nanotube to hydroalcoholic solution, adding resorcinol, formaldehyde, sodium carbonate and silver nanowires to obtained solution under ultrasonic condition to obtain mixed solution, reacting mixed solution at 70-80 degrees C for 48-96 hours to obtain gel, freeze-drying obtained gel at (-50)-(-30) degrees C for 48-96 hours to obtain aerogel, carrying out heat treatment with aerogel at 200-400 degrees C and carrying out secondary heat treatment at 650-750 degrees C.