• 专利标题:   Preparation of nitrogen doped reduced graphene oxide for electrochemical energy storage, involves heating aqueous mixture of graphene oxide and glycine, centrifuging resulting black suspension, and drying resulting sample under vacuum.
  • 专利号:   IN201811031021-A
  • 发明人:   KUMAR A, THAREJA S
  • 专利权人:   INDIAN INST TECHNOLOGY
  • 国际专利分类:   H01G011/00
  • 专利详细信息:   IN201811031021-A 03 Jul 2020 H01G-011/00 202065 Pages: 29 English
  • 申请详细信息:   IN201811031021-A IN11031021 20 Aug 2018
  • 优先权号:   IN11031021

▎ 摘  要

NOVELTY - Preparation of nitrogen doped reduced graphene oxide (N-rGO) involves heating aqueous mixture of graphene oxide and glycine under non-corrosive conditions, adjusting pH to 6-9, preferably 8, aging for 0.5-2 hours, preferably 1 hour at room temperature, heating at 70-100 degrees C, preferably 95 degrees C for 6-16 hours, preferably 12 hours, centrifuging resulting black suspension and repeatedly washing with deionized water to remove any residual precursors, and drying resulting sample under vacuum at 50-70 degrees C for 8-16 hours, preferably 60 degrees C for 12 hours. USE - Preparation of nitrogen doped reduced graphene oxide used for electrochemical energy storage such as battery, supercapacitor (all claimed) and fuel cell. ADVANTAGE - The method ensures greener wet synthesis of nitrogen-doped reduced graphene oxide (N-rGO), is economical, and produces environmentally-friendly electrolytic components. The process is carried out using greener reducing agents under mold conditions. The nitrogen-doped reduced graphene oxide produces high performance supercapacitor with long cyclability and high energy density.