• 专利标题:   Preparing modified graphene oxide comprises preparing graphene oxide by Hummers method, reacting aminopropyltriethoxysilane with graphene oxide, and subjecting to surface-initiated atom transfer radical polymerization.
  • 专利号:   CN110182795-A
  • 发明人:   MA L, LUO P, HE Y, FAN Y, ZHANG L, PENG X
  • 专利权人:   UNIV SOUTHWEST PETROLEUM
  • 国际专利分类:   C01B032/194, C01B032/198, C09K008/03
  • 专利详细信息:   CN110182795-A 30 Aug 2019 C01B-032/198 201973 Pages: 15 Chinese
  • 申请详细信息:   CN110182795-A CN10355919 29 Apr 2019
  • 优先权号:   CN10355919

▎ 摘  要

NOVELTY - Preparing modified graphene oxide comprises (i) preparing graphene oxide (GO) by Hummers method, (ii) reacting aminopropyltriethoxysilane (APTES) with graphene oxide to obtain APTES-GO, (iii) reacting bromine-containing initiator with the APTES-GO obtained in the step (ii) under the action of catalyst to obtain graphene oxide- aminopropyltriethoxysilane-bromide (GO-APTES-Br), and(iv) selecting monomer having hydrophilic group, taking monomer and the GO-APTES-Br obtained in the step (iii), subjecting to surface-initiated atom transfer radical polymerization under the action of catalyst to obtain graphene oxide surface graft polymer. USE - The method is useful for preparing modified graphene oxide. ADVANTAGE - The method provides stable dispersion in a high temperature, high salt and weakly alkaline solution, especially for stable dispersion in a working fluid during oil and gas production.