• 专利标题:   Method for preparing tin dioxide-oxidized bacterial cellulose/reduced graphene oxide electrode material comprises e.g. dissolving tin chloride in concentrated hydrochloric acid, oxidizing bacterial cellulose slurry and centrifuging product.
  • 专利号:   CN112768655-A, CN112768655-B
  • 发明人:   QIAN C, JIA P, JIN S, XU L, LI C, NIU Y, LI J, HAN Q, HANG J, MA X, WANG X, ZHANG R, JIN M
  • 专利权人:   SHANGHAI INST TECHNOLOGY
  • 国际专利分类:   B82Y040/00, H01M010/0525, H01M004/36, H01M004/48, H01M004/62
  • 专利详细信息:   CN112768655-A 07 May 2021 H01M-004/36 202146 Pages: 6 Chinese
  • 申请详细信息:   CN112768655-A CN10029725 11 Jan 2021
  • 优先权号:   CN10029725

▎ 摘  要

NOVELTY - The method comprises (1) dissolving tin chloride in concentrated hydrochloric acid to form a stable acidic tin chloride solution, (2) oxidizing the bacterial cellulose slurry through 2,2,6,6-tetramethylpiperidine oxide to obtain oxidized bacterial cellulose (OBC), and configuring into an oxidized bacterial cellulose solution, (3) mixing the acidic tin chloride solution, oxidized bacterial cellulose solution, and graphene oxide dispersion in a hydrothermal kettle, stirring to form a uniform mixed solution, and performing hydrothermal treatment, and (4) cooling the hydrothermal kettle to room temperature, centrifuging the product, washing with water and ethanol, and freeze-drying. USE - Method for preparing tin dioxide-oxidized bacterial cellulose/reduced graphene oxide electrode material. ADVANTAGE - The method is simple and environmentally friendly, and has low energy consumption. The electrode material has excellent electrochemical performance.