• 专利标题:   Preparing oxidation-resistant elastic graphene airgel comprises e.g. soaking elastic graphene aerogel in condensed ring aromatic compound solution, water activation and freeze-drying, atomic layer deposition, annealing, soaking in polydimethylsiloxane solution, and curing and vacuum heat treatment.
  • 专利号:   CN115650221-A
  • 发明人:   HUANG H, WANG P, ZHANG E, CHENG P, LIU Y, LI W, ZHANG W
  • 专利权人:   AEROSPACE SPECIAL MATERIALS PROCESSING
  • 国际专利分类:   B01J013/00, C01B032/194
  • 专利详细信息:   CN115650221-A 31 Jan 2023 C01B-032/194 202322 Chinese
  • 申请详细信息:   CN115650221-A CN11339192 28 Oct 2022
  • 优先权号:   CN11339192

▎ 摘  要

NOVELTY - Preparing oxidation-resistant elastic graphene airgel comprises (a) soaking the elastic graphene aerogel in the condensed ring aromatic compound solution to obtain a graphene wet gel, (b) carrying out water activation and freeze-drying to obtain modified graphene airgel, (c) subjecting modified graphene airgel to atomic layer deposition to obtain a modified graphene airgel with a thin layer of aluminum oxide deposited on the surface, and thermal annealing under an inert atmosphere to obtain an aluminum oxide/graphene gas gel, and (d) soaking the alumina/graphene airgel in the polydimethylsiloxane (PDMS) solution, and performing curing and vacuum heat treatment. USE - The method is useful for preparing oxidation-resistant elastic graphene airgel. ADVANTAGE - The anti-oxidation elastic graphene airgel has superelastic properties at room temperature, can still maintain high elasticity in a high-temperature aerobic environment at 1300℃, greatly improves the temperature resistance of graphene airgel to 1300℃ in an aerobic environment.