• 专利标题:   Preparing cuprous oxide composite film involves preparing sodium alginate aqueous solution and copper salt solution, and then adding graphene into copper salt solution under microwave conditions with stirring to obtain mixed solution.
  • 专利号:   CN105561403-A, CN105561403-B
  • 发明人:   GUO P, LI Q, LI Z, SHANG K, XIA Y, WANG Y, ZHAO X, SUN X
  • 专利权人:   UNIV QINGDAO
  • 国际专利分类:   A61L015/18, A61L015/28, A61L015/42, A61L015/44, A61L031/02, A61L031/04, A61L031/14, A61L031/16
  • 专利详细信息:   CN105561403-A 11 May 2016 A61L-031/04 201645 Pages: 8 English
  • 申请详细信息:   CN105561403-A CN10116368 02 Mar 2016
  • 优先权号:   CN10116368

▎ 摘  要

NOVELTY - Cuprous oxide composite film preparation involves preparing 2-7 mass% sodium alginate aqueous solution and 10 mass% copper salt solution, and then adding graphene into copper salt solution under microwave conditions with stirring at high speed for 30-120 minutes to obtain a mixed solution. The graphene mixed solution is slowly added into the sodium alginate aqueous solution in a molar ratio of 1:1-1.5 at 20-100 degrees C, where glucose or ascorbic acid as a reducing agent is also added with stirring for 30-60 minutes to obtain alginate-graphene copper oxide gel. USE - Method for preparing cuprous oxide composite film (claimed) for use as a band-aid and other medical materials. ADVANTAGE - The method prepares the cuprous oxide composite film in a simple manner with uniform internal structure, controllable particle size, good water absorption and permeability and broad market prospects. DETAILED DESCRIPTION - Cuprous oxide composite film preparation involves preparing 2-7 mass% sodium alginate aqueous solution and 10 mass% copper salt solution, and then adding graphene into copper salt solution under microwave conditions with stirring at high speed for 30-120 minutes to obtain a mixed solution. The graphene mixed solution is slowly added into the sodium alginate aqueous solution in a molar ratio of 1:1-1.5 at 20-100 degrees C, where glucose or ascorbic acid as a reducing agent is also added with stirring for 30-60 minutes to obtain alginate-graphene copper oxide gel. The resulting gel is defoamed in vacuum and then aged for 24-48 hours to give casting solution, where the casting solution is extruded in a mold to give the cuprous oxide composite film. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic electron micrograph of the cuprous oxide composite film.