• 专利标题:   Preparing cobalt (II) oxide/reduced graphene oxide composite negative electrode material involves adding oleylamine and oleic acid into isopropanol in certain volume ratio to obtain solution A, adding cobalt source and precipitating agent.
  • 专利号:   CN107256951-A
  • 发明人:   CAO L, KANG Q, CUI Y, LI J, HUANG J, CHENG Y
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, H01M004/36, H01M004/525, H01M004/587, H01M004/62
  • 专利详细信息:   CN107256951-A 17 Oct 2017 H01M-004/36 201773 Pages: 12 Chinese
  • 申请详细信息:   CN107256951-A CN10429276 08 Jun 2017
  • 优先权号:   CN10429276

▎ 摘  要

NOVELTY - Preparing cobalt (II) oxide/reduced graphene oxide composite negative electrode material involves adding oleylamine and oleic acid into isopropanol in volume ratio of (0.5-2):(0.5-2):80 to obtain solution A. The cobalt source and precipitating agent are added into solution A, and stirring to obtain solution B, where ratio of cobalt source and isopropanol solution is (1~5) mmol:80 milliliter. USE - Method for preparing cobalt (II) oxide/reduced graphene oxide composite negative electrode material (claimed). ADVANTAGE - The method enables to prepare cobalt (II) oxide/reduced graphene oxide composite negative electrode material which has improves specific capacity of the electrode, generates fly catching grass-like compound which has great help to maintain stability of the material, reduces volume expansion effect of material, improves auxiliary effect of conductivity, and has improve electrochemical performance of the material. DETAILED DESCRIPTION - Preparing cobalt (II) oxide/reduced graphene oxide composite negative electrode material involves adding oleylamine and oleic acid into isopropanol in volume ratio of (0.5-2):(0.5-2):80 to obtain solution A. The cobalt source and precipitating agent are added into solution A, and stirring to obtain solution B, where ratio of cobalt source and isopropanol solution is (1~5) mmol:80 milliliter. The graphene oxide is added into solution B, stirred uniformly to obtain suspension C, where ratio of graphene oxide to isopropanol solution is (0.08-0.24) gram: 80 milliliter. The suspension C is sonicated undergoes oil bath reaction to obtain precipitate. The precipitate is separated, washed, and dried to obtain precursor. The precursor is incubated in atmosphere furnace at 300-500 degrees C for 0.5-2 hours, cooled to room temperature to obtain final product.