• 专利标题:   Preparation of continuous macroscopic graphene nanoribbon fiber for wearable electronic device, involves ultrasonically mixing carbon-containing compound, ferrocene and thiophene, adding deionized water, injecting reaction liquid, spinning.
  • 专利号:   CN108751174-A
  • 发明人:   KANG Y, LI Z, XU K, HE X, CAO Y, LI Y
  • 专利权人:   UNIV QUJING NORMAL
  • 国际专利分类:   C01B032/186, D01F009/127
  • 专利详细信息:   CN108751174-A 06 Nov 2018 C01B-032/186 201901 Pages: 11 Chinese
  • 申请详细信息:   CN108751174-A CN10704525 01 Jul 2018
  • 优先权号:   CN10704525

▎ 摘  要

NOVELTY - Preparation of continuous macroscopic graphene nanoribbon fiber, involves using high-hydrogen reaction liquid as a raw material prepared directly by chemical vapor deposition. The method involves (1) using liquid carbon-containing compound, ferrocene, thiophene and deionized water as raw materials, mixing carbon-containing compound, ferrocene and thiophene in a mass ratio of 50-300:1-5:1, adding 15-40 %mass, preferably 20-35 %mass deionized water, ultrasonically mixing, injecting reaction liquid into tubular reactor at 700-1500 degrees C and 5-20 mL/hour under hydrogen carrier gas flow of 200-2000 sccm, growing and assembling to form continuous graphene nanoribbon aggregate, (2) pulling the graphene nanoribbon aggregates from the end of the reactor, compacting by liquid phase and spinning at 2-20 m/minute. USE - Preparation of continuous macroscopic graphene nanoribbon fiber for flexible wearable electronic device. ADVANTAGE - The method enables simple and large-scale preparation of uniformly continuous lightweight macroscopic graphene nanoribbon fiber with high purity, high quality, high strength, high electrical conductivity and excellent flexibility, and adopts one-step dry spinning.