• 专利标题:   Preparing thermally conductive graphene film involves immersing graphite in mixed acid solution, and adding intercalating agent under stirring to obtain mixed solution, which is added with organic reagent.
  • 专利号:   CN105964522-A, CN105964522-B
  • 发明人:   NIU L, WU T
  • 专利权人:   CHANGCHUN APPLIED CHEM INST CHINESE ACAD, CHANGCHUN APPLIED CHEM INST CHINESE ACAD
  • 国际专利分类:   B05D003/02, B05D007/04, B05D007/14, C04B035/52, C04B035/536, C04B035/622
  • 专利详细信息:   CN105964522-A 28 Sep 2016 B05D-007/14 201682 Pages: 9 Chinese
  • 申请详细信息:   CN105964522-A CN10292668 05 May 2016
  • 优先权号:   CN10292668

▎ 摘  要

NOVELTY - Preparing thermally conductive graphene film involves immersing graphite in mixed acid solution, and adding intercalating agent under stirring to obtain mixed solution. The obtained mixed solution is added with organic reagent to obtain aqueous dispersion of graphene. The aqueous dispersion of graphene is added with natural long fiber or polymer long fiber to obtain mixture, which is subjected to supercritical ultrasonic treatment to obtain mixed dispersion liquid. The mixed dispersion liquid is applied on substrate, which is then dried at 500-900 degrees C for 15-30 minutes. USE - Method for preparing thermally conductive graphene film (claimed). ADVANTAGE - The method enables to prepare thermally conductive graphene film, which has high degree of orientation, 1000-1500W/mK thermal conductivity and 3070 megapascals mechanical tensile strength. DETAILED DESCRIPTION - Preparing thermally conductive graphene film involves immersing graphite in mixed acid solution, and adding intercalating agent under stirring to obtain mixed solution. The obtained mixed solution is added with organic reagent to obtain aqueous dispersion of graphene. The aqueous dispersion of graphene is added with natural long fiber or polymer long fiber to obtain mixture, which is subjected to supercritical ultrasonic treatment to obtain mixed dispersion liquid. The mixed dispersion liquid is applied on substrate, which is then dried at 500-900 degrees C for 15-30 minutes to obtain thermally conductive graphene film.