• 专利标题:   Preparation of graphene oxide by stirring concentrated sulfuric acid, graphite, potassium nitrate and potassium permanganate, heating, adding distilled water and hydrogen peroxide, standing, centrifuging, washing, dispersing and drying.
  • 专利号:   CN105565299-A
  • 发明人:   LIU Q
  • 专利权人:   SHAANXI GAOHUA ZHIBEN CHEM TECHNOLOGY CO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN105565299-A 11 May 2016 C01B-031/04 201657 Pages: 4 English
  • 申请详细信息:   CN105565299-A CN10835279 26 Nov 2015
  • 优先权号:   CN10835279

▎ 摘  要

NOVELTY - Preparation of graphene oxide comprises adding concentrated sulfuric acid to beaker, controlling temperature at 10-15 degrees C, gradually adding 1.6 g graphite, 1.6 g potassium nitrate and 9.0 g potassium permanganate, stirring, heating for 10 minutes, heating to 40 degrees C, adding 120 mL distilled water, heating to 45 degrees C, adding 300 mL distilled water and hydrogen peroxide solution, changing color into bright yellow, standing to precipitate, centrifuging, water washing to neutral, adding water, ultrasonically dispersing, placing in culture dish and drying to constant weight in drying box. USE - Method for preparing graphene oxide (claimed). ADVANTAGE - The graphene oxide has large amount of oxygen-containing reactive groups, high degree of peeling, crystalline structure and high activity. The method has simple steps and easy operation.