• 专利标题:   Multi-edge molybdenum disulfide nanosheets/graphene nano-composite material, comprises graphene and multi-edge molybdenum disulfide nanosheets.
  • 专利号:   CN104091931-A, CN104091931-B
  • 发明人:   CHEN Q, CHEN T, CHEN W, MA L, SUN H, YE J, WU Q
  • 专利权人:   UNIV ZHEJIANG
  • 国际专利分类:   B82Y030/00, B82Y040/00, H01M004/36
  • 专利详细信息:   CN104091931-A 08 Oct 2014 H01M-004/36 201502 Pages: 9 Chinese
  • 申请详细信息:   CN104091931-A CN10339879 17 Jul 2014
  • 优先权号:   CN10339879

▎ 摘  要

NOVELTY - A multi-edge molybdenum disulfide nanosheets/graphene nano-composite material comprises graphene and multi-edge molybdenum disulfide nanosheets at a ratio of 1:1-1:4. USE - Multi-edge molybdenum disulfide nanosheets/graphene nano-composite material. ADVANTAGE - The composite material has wide application effect, and is simple, convenient and easy to prepare. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a method for preparing a multi-edge molybdenum disulfide nanosheets/graphene nano-composite material, which involves dispersing graphene oxide in deionized water ultrasonically, followed by adding 5-25 ml/l ionic liquid comprising 1-butyl-3-methylimidazolium tetrafluoroborate, adding L- cysteine and sodium at a ratio of 5:1 to obtain mixed solution, transferring the mixed solution to a hydrothermal reaction kettle, adjusting volume to 80% by adding deionized water to carry out hydrothermal reaction, placing the resultant solution in a thermostatic oven to perform hydrothermal reaction at 240 degrees C for 24 hours, naturally cooling, and centrifuging to obtain solid product, rinsing the solid product in hot water, washing and drying at 100 degrees C under vacuum, performing hydrothermal treatment on the solid product in a nitrogen/hydrogen mixed atmosphere at 500 degrees C for 2 hours, 10% hydrogen mixed gas, and preparing multi-edge molybdenum disulfide nanosheets/ graphene composite nanomaterial.