• 专利标题:   Preparation of flax-based carboxymethylcellulose and oxidized graphene composite film involves mixing carboxymethylcellulose solution and graphene suspension, ultrasonically dispersing, degassing, casting and drying.
  • 专利号:   CN106317433-A
  • 发明人:   DONG F, LIU Z
  • 专利权人:   UNIV QIQIHAR
  • 国际专利分类:   C08B011/12, C08J005/18, C08K003/04, C08L001/28
  • 专利详细信息:   CN106317433-A 11 Jan 2017 C08J-005/18 201728 Pages: 6 Chinese
  • 申请详细信息:   CN106317433-A CN10679633 13 Aug 2016
  • 优先权号:   CN10679633

▎ 摘  要

NOVELTY - Preparation of flax-based carboxymethylcellulose and oxidized graphene composite film involves mixing carboxymethylcellulose solution and graphene suspension, ultrasonically dispersing for 10 minutes, magnetically stirring for 60 minutes, forming mixed solution, degassing resultant mixed solution in vacuum degassing machine under vacuum degree of 0.09 MPa, casting obtained mixture in culture dish, and drying at room temperature for 48 hours. USE - Preparation of flax-based carboxymethylcellulose and oxidized graphene composite film (claimed). ADVANTAGE - The method efficiently provides flax-based carboxymethylcellulose and oxidized graphene composite film having excellent adsorption performance. DETAILED DESCRIPTION - Preparation of flax-based carboxymethylcellulose and oxidized graphene composite film involves placing 0.2 g graphene oxide in ultrasonic cell crushing cup, adding 50 ml distilled water, ultrasonically crushing for 3 hours, forming 4 mg/ml oxidized graphene suspension, dissolving 2 g carboxymethyl cellulose in 100 ml distilled water, adding 1 ml glycerol, magnetically stirring in constant temperature water bath at 65 degrees C for 30 minutes, forming 2 %mass homogeneous stable carboxymethylcellulose solution, mixing obtained carboxymethylcellulose solution and graphene suspension in the ratio of 2:1, 4:1 or 8:1, ultrasonically dispersing for 10 minutes, magnetically stirring for 60 minutes, forming mixed solution, degassing resultant mixed solution in vacuum degassing machine under vacuum degree of 0.09 MPa, casting obtained mixture in culture dish, and drying at room temperature for 48 hours.