• 专利标题:   Preparation of micro-arc oxidation film-zeolitic imidazolate framework-8-graphene oxide/layered double hydroxides film on surface of magnesium alloy used e.g. for aviation, involves carrying out micro-arc oxidation, washing and drying.
  • 专利号:   CN113355717-A, CN113355717-B
  • 发明人:   WU L, CHEN Y, YAO W, WU J, PAN F
  • 专利权人:   UNIV CHONGQING
  • 国际专利分类:   C25D011/30, C23C026/00
  • 专利详细信息:   CN113355717-A 07 Sep 2021 C25D-011/30 202181 Pages: 22 Chinese
  • 申请详细信息:   CN113355717-A CN10624044 04 Jun 2021
  • 优先权号:   CN10624044

▎ 摘  要

NOVELTY - Preparation of micro-arc oxidation film-zeolitic imidazolate framework-8-graphene oxide/layered double hydroxides film on surface of magnesium alloy comprises carrying out micro-arc oxidation to surface of magnesium alloy to form film, putting magnesium alloy after micro-arc oxidation into graphene oxide growth liquid solution for in-situ growth, reacting at 125-145 degrees C with pH value of 9-12.5 for 10-20 hours, putting in mixed solution of dimethylimidazole and zinc nitrate hexahydrate to grow in situ, reacting at room temperature for 5-35 hours, ultrasonically cleaning magnesium alloy after reaction, using deionized water to wash, and drying to obtain product. USE - The method is used for preparing micro-arc oxidation film-zeolitic imidazolate framework-8-graphene oxide/layered double hydroxides film on surface of magnesium alloy for aviation, automobile, and electronic communication (claimed). ADVANTAGE - The method enables to prepare magnesium alloy surface micro-arc oxidation film-8-graphene oxide/ZIF composite film in a simple and eco-friendly manner.