• 专利标题:   Preparation of nitrogen-doped pore graphene loaded with cobalt involves preparing graphene aerogel containing ascorbic acid, dialyzing, immersing in polyacrylic acid solution, heating, immersing in cobalt chloride, heating, and calcining.
  • 专利号:   CN110217780-A
  • 发明人:   CHEN Y, CAO K, BAI J
  • 专利权人:   UNIV SHAANXI NORMAL
  • 国际专利分类:   B01J027/24, C01B032/184
  • 专利详细信息:   CN110217780-A 10 Sep 2019 C01B-032/184 201978 Pages: 10 Chinese
  • 申请详细信息:   CN110217780-A CN10538113 20 Jun 2019
  • 优先权号:   CN10538113

▎ 摘  要

NOVELTY - Preparation of nitrogen-doped pore graphene loaded with cobalt involves mixing aqueous dispersion of graphene oxide, and ascorbic acid, heating at 70-100 degrees C for 1-5 hours to obtain graphene aerogel, dialyzing graphene aerogel in ultrapure water, immersing in polyacrylic acid aqueous solution, heating at 60-120 degrees C for 1-5 hours, preferably 80-100 degrees C for 2-4 hours, removing from the solution, dialyzing in ultrapure water, immersing in aqueous solution of cobalt chloride, heating at 60-120 degrees C for 1-5 hours, preferably 80-100 degrees C for 2-4 hours, lyophilizing, and calcining at 700-1000 degrees C. USE - Preparation of nitrogen-doped pore graphene loaded with cobalt. ADVANTAGE - The nitrogen-doped pore graphene loaded with cobalt has unique structure, excellent stability, and excellent oxygen reduction reaction catalytic activity and stability in alkaline potassium hydroxide solution. The nitrogen-doped pore graphene loaded with cobalt is prepared by simple, and economical method.