• 专利标题:   Manufacture of graphene nanoribbon involves etching metal substrate, heating, irradiating UV ray, processing with protective gas, mixing with chloride intercalation agent and ionic liquid, placing in magnetic field and filtering.
  • 专利号:   CN103935982-A, CN103935982-B
  • 发明人:   WANG Y, WU F, YUAN X, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING ENG CO LTD, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   B82Y030/00, C01B031/04
  • 专利详细信息:   CN103935982-A 23 Jul 2014 C01B-031/04 201468 Pages: 15 Chinese
  • 申请详细信息:   CN103935982-A CN10019484 18 Jan 2013
  • 优先权号:   CN10019484

▎ 摘  要

NOVELTY - Manufacture of graphene nanoribbon involves placing metal substrate in acid having concentration of 0.01-1 mol/L, etching for 0.5-10 minutes, heating at 600-900 degrees C under anaerobic condition, irradiating UV ray, processing using protective gas and carbon-containing gas for 30-300 minutes, obtaining metal substrate surface containing carbon nanowall, mixing resultant carbon nanowall and chloride intercalation agent in the ratio of 1:0.8-1.2, heating at 460-550 degrees C for 2-6 hours, mixing with ionic liquid, placing resultant mixture in constant magnetic field and filtering. USE - Manufacture of graphene nanoribbon (claimed). ADVANTAGE - The method enables preparation of graphene nanoribbon having high electroconductivity. DETAILED DESCRIPTION - Manufacture of graphene nanoribbon involves placing metal substrate in acid having concentration of 0.01-1 mol/L, etching for 0.5-10 minutes, heating at 600-900 degrees C under anaerobic condition, irradiating UV ray, processing using protective gas and carbon-containing gas for 30-300 minutes, obtaining metal substrate surface containing carbon nanowall, mixing resultant carbon nanowall and chloride intercalation agent in the ratio of 1:0.8-1.2, heating at 460-550 degrees C for 2-6 hours, mixing with ionic liquid, placing resultant mixture in constant magnetic field with magnetic strength of 0.01-1 tesla and filtering. The flow rate of carbon-containing gas is 10-1000 sccm. The ratio of carbon-containing gas and protective gas is 2-10:1.