• 专利标题:   Preparation of cuprous oxide/graphene oxide visible light catalyst used for organic wastewater treatment, involves taking commercial graphite, potassium permanganate and concentrated sulfuric acid, mixing, reacting, and cooling.
  • 专利号:   CN107790129-A
  • 发明人:   HE D, WANG J, JIN C, LIN L
  • 专利权人:   NAT ENG RES CENT NANOTECHNOLOGY
  • 国际专利分类:   B01J023/72, C02F001/30, C02F101/30
  • 专利详细信息:   CN107790129-A 13 Mar 2018 B01J-023/72 201826 Pages: 7 Chinese
  • 申请详细信息:   CN107790129-A CN11065018 02 Nov 2017
  • 优先权号:   CN11065018

▎ 摘  要

NOVELTY - A cuprous oxide/graphene oxide visible light catalyst is prepared by taking commercial graphite, potassium permanganate and concentrated sulfuric acid, mixing, reacting, cooling, adding water, stirring, adding hydrogen peroxide, stirring, separating solid, washing solid product, freeze drying to obtain graphene oxide, taking hydrated copper acetate, dissolving in deionized water, adding graphene oxide, stirring, adding sodium hydroxide solution, centrifuging, adding sugar compound solution, stirring, carrying out hydrothermal reaction, taking solid product, washing, and drying. USE - Method for preparing cuprous oxide/graphene oxide visible light catalyst used for organic wastewater treatment (claimed). ADVANTAGE - The catalyst has electronic capture good transmission performance, has reduced cuprous oxide photogenerated electron recombination rate and has high photocatalytic efficiency. DETAILED DESCRIPTION - A cuprous oxide/graphene oxide visible light catalyst is prepared by taking commercial graphite, potassium permanganate and concentrated sulfuric acid, mixing at - 4? to 0 degrees C for 1 hour, reacting for 1-12 hours at 70-120 degrees C, cooling, adding water, stirring, adding hydrogen peroxide, stirring, separating out solid product, washing solid product to pH value of 7, freeze drying to obtain graphene oxide, taking hydrated copper acetate, dissolving in deionized water to prepare 1.0 mol/L solution, adding graphene oxide, stirring, adding sodium hydroxide solution, centrifuging, adding sugar compound solution, stirring, carrying out hydrothermal reaction at 70-110 degrees C for 12 hours, taking solid product, washing, and drying.