• 专利标题:   Luminous composite material comprises cyanoethylchitosan, acrylic acid ester-styrene copolymer, n-butyl lithium, sulfoacetamide, trimethylsiloxy silicate, ceramic powder, hexadecanoic acid, graphene, N-formylmorpholine and europium chloride.
  • 专利号:   CN104962021-A
  • 发明人:   DANG B
  • 专利权人:   SUZHOU KEMIAO NEW MATERIALS CO LTD
  • 国际专利分类:   C08K013/02, C08K003/04, C08K003/16, C08K003/22, C08K003/36, C08K003/38, C08K005/56, C08L033/08, C08L005/08, C09K011/02, C09K011/06
  • 专利详细信息:   CN104962021-A 07 Oct 2015 C08L-033/08 201602 Pages: 7 Chinese
  • 申请详细信息:   CN104962021-A CN10409880 14 Jul 2015
  • 优先权号:   CN10409880

▎ 摘  要

NOVELTY - Luminous composite material comprises 10-20 pts. wt. cyanoethylchitosan, 60-80 pts. wt. acrylic acid ester-styrene copolymer, 8-10 pts. wt. n-butyl lithium, 15-22 pts. wt. sulfo-acetamide, 6-8 pts. wt. trimethylsiloxy silicate, 16-22 pts. wt. ceramic powder, 2-3 pts. wt. hexadecanoic acid, 2-5 pts. wt. graphene, 1-1.5 pts. wt. N-formylmorpholine, and 0.5-1.1 pts. wt. europium(III) chloride; acrylate-styrene copolymer molecular weight is 20000-34000; the molecular weight of cyanoethylchitosan is 5000-11000; the ceramic powder raw material comprises e.g. 25% silicon dioxide. USE - Used as luminous composite material. ADVANTAGE - The method uses widely available raw material source, has simple and controllable preparation process, is easy to operate, and is suitable for industrialization. DETAILED DESCRIPTION - Luminous composite material comprises 10-20 pts. wt. cyanoethylchitosan, 60-80 pts. wt. acrylic acid ester-styrene copolymer, 8-10 pts. wt. n-butyl lithium, 15-22 pts. wt. sulfo-acetamide, 6-8 pts. wt. trimethylsiloxy silicate, 16-22 pts. wt. ceramic powder, 2-3 pts. wt. hexadecanoic acid, 2-5 pts. wt. graphene, 1-1.5 pts. wt. N-formylmorpholine, and 0.5-1.1 pts. wt. europium(III) chloride, obtained by mold pressing; acrylate-styrene copolymer molecular weight is 20000-34000; the molecular weight of cyanoethylchitosan is 5000-11000; the ceramic powder raw material comprises 25% silicon dioxide, 15% ytterbium fluoride, 20% boron oxide, 15% rutile type titanium dioxide, 10% magnesium oxide, and 10% shell powder. An INDEPENDENT CLAIM is also included for preparing luminous composite material comprising mixing europium(III) chloride, trimethylsiloxy silicate for 2 hours, obtaining mixture, sequentially adding sulfo-acetamide, ceramic powder and mixture, stirring for 4 hours, then adding palmitic acid, normal-butyl lithium, stirring at 80 degrees C for 2 hours, adding cyanoethylchitosan, graphene, stirring at 120 degrees C for 1 hour, adding acrylic ester-styrene copolymer, N-formyl morpholine, stirring at 130 degrees C for 4 hours to obtain luminous composite material.