• 专利标题:   Preparing chitosan-packaged nano-silver graphene oxide composite antibacterial material involves mixing silver nitrate solution and O-carboxymethyl chitosan solution, where mixed solution is stirred in quartz cuvette at room temperature.
  • 专利号:   CN106417275-A
  • 发明人:   WEI L, NIU B, ZHANG J, GUAN L, MA S, LIU R
  • 专利权人:   UNIV TAIYUAN TECHNOLOGY
  • 国际专利分类:   A01N025/08, A01N059/16, A01P001/00, A01P003/00
  • 专利详细信息:   CN106417275-A 22 Feb 2017 A01N-025/08 201732 Pages: 6 Chinese
  • 申请详细信息:   CN106417275-A CN10736601 29 Aug 2016
  • 优先权号:   CN10736601

▎ 摘  要

NOVELTY - Preparing chitosan-packaged nano-silver graphene oxide composite antibacterial material involves mixing 0.1 wt.% silver nitrate solution and 0.1 wt.% O-carboxymethyl chitosan solution in volume ratio of 20:80-1:99. The mixed solution is stirred in 4mL quartz cuvette at room temperature for 0.5-1 hours. The stirred material is sealed in presence of nitrogen. The sealed quartz cuvette is irradiated with ultraviolet lamp for 15 minutes. The mixed solution is stirred with anhydrous ethanol for 60 minutes to obtain precipitate that is washed for two times with 50% ethanol. USE - Method for preparing chitosan-packaged nano-silver graphene oxide composite antibacterial material (claimed). ADVANTAGE - The method enables to prepare chitosan-packaged nano-silver graphene oxide composite antibacterial material that ensures no chemical additive content, reduced toxicity of antibacterial agent, good antibacterial effect, no harm to human body, low cost and green and environment-friendly preparation method. DETAILED DESCRIPTION - Preparing chitosan-packaged nano-silver graphene oxide composite antibacterial material involves mixing 0.1 wt.% silver nitrate solution and 0.1 wt.% O-carboxymethyl chitosan solution in volume ratio of 20:80-1:99. The mixed solution is stirred in 4mL quartz cuvette at room temperature for 0.5-1 hours. The stirred material is sealed in presence of nitrogen. The sealed quartz cuvette is irradiated with ultraviolet lamp for 15 minutes. The mixed solution is stirred with anhydrous ethanol for 60 minutes to obtain precipitate that is washed for two times with 50% ethanol. The washed precipitate is dissolved in ultra-pure water. The obtained solution is processed ultrasonically for 5-10 minutes to obtain O-carboxymethyl chitosan nano-silver dispersion liquid that is mixed with graphene oxide dispersion liquid in volume ratio of 1:5-5:1 ultrasonically for 5-10 minutes to obtain product.