• 专利标题:   Preparation of aperture controllable three-dimensional graphene involves cooling graphite powder, adding concentrated sulfuric acid and sodium nitrate, stirring, reacting, adding potassium permanganate, heating, reacting and cooling.
  • 专利号:   CN104163424-A, CN104163424-B
  • 发明人:   GUO X, LI Q, ZHANG L, ZHANG Y, HAO W, WANG Y
  • 专利权人:   UNIV SOUTHEAST
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104163424-A 26 Nov 2014 C01B-031/04 201507 Pages: 5 Chinese
  • 申请详细信息:   CN104163424-A CN10405237 15 Aug 2014
  • 优先权号:   CN10405237

▎ 摘  要

NOVELTY - Preparation of aperture controllable three-dimensional graphene comprises cooling graphite powder, adding concentrated sulfuric acid and sodium nitrate, stirring for 5-15 minutes, reacting, adding potassium permanganate, heating to 40-60 degrees C, adding deionized water, reacting, cooling, centrifuging, washing, dissolving, filtering, soaking in polymethyl methacrylate, drying, adding hydroiodic acid, reacting for 0.5-3 hours, washing with deionized water, soaking ammonium persulfate solution, dissolving, cleaning, drying, purging, heating at 300-500 degrees C for 0.5-3 hours and cooling. USE - Method for preparing aperture controllable three-dimensional graphene (claimed). ADVANTAGE - The graphene has good absorbing property and conductivity.